Sodium Methoxide → HCID 13958463, compound

Participants

Reaction Steps

Using the method of Example 157, 4-chloro-1-(2,3-dihydroxypropyl)-1H-imidazo[4,5-c]quinoline (from Example 124, Part D) was reacted with sodium methoxide to provide 1-(2,3-dihydroxypropyl)-4-methoxy-1H-imidazo[4,5-c]quinoline, m.p. 214°-216° C. after recrystallization from isopropanol. Analysis: Calculated for C14H15N3O3 : %C, 61.5; %H, 5.5; N, 15.4; Found: %C, 61.3; %H, 5.5; %N, 15.4.

Provenance & Evidence