Benzyl Chloride → HCID 13958468, compound

Participants

Reaction Steps

Using the method of Example 162, 2-mercapto-1-methyl-1H-imidazo[4,5-c]quinoline (from Example 165 below) was reacted with benzyl chloride to provide 2-benzylthio-1-methyl-1H-imidazo[4,5-c]quinoline. Recrystallization first from isopropanol then from ethanol provided solid product, m.p. 160°-163° C. Analysis: Calculated for C18H15N3S: %C, 70.8; %H, 5.0; %N, 13.8. Found: %C, 70.3; %H, 4.7; %N, 13.7.

Provenance & Evidence