HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 13986496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 2-Chloro-N-{2-[methyl(phenyl)amino]pyridin-3-yl}benzamide | HCID 13560186 | — |
| Product | HCID 13986496 | HCID 13986496 | — |
Reaction Steps
Following the procedure of Example 58, 2-chloro-N-[2-(methylphenylamino)-3-pyridinyl]benzamide was cyclized to the title compound with phosphorus oxychloride and isolated, recrystallizing from isopropyl alcohol as yellow solid, m.p. 131.5°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698430 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-ea92c5b1c201434aa95ab131c23fc83e |
| Source note | uspto-grants-1987_10 |