HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → N-(2-dimethylaminoethyl)-6-methyl-4-(3-nitrophenyl)-2-phenyl-5-pyrimidinecarboxamide fumarate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | N-(2-dimethylaminoethyl)-6-methyl-4-(3-nitrophenyl)-2-phenyl-5-pyrimidinecarboxamide | HCID 10319094 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(2-dimethylaminoethyl)-6-methyl-4-(3-nitrophenyl)-2-phenyl-5-pyrimidinecarboxamide fumarate | HCID 20183348 | — |
Reaction Steps
To the solution of N-(2-dimethylaminoethyl)-6-methyl-4-(3-nitrophenyl)-2-phenyl-5-pyrimidinecarboxamide (4 g) in ethyl alcohol (10 ml), the solution of fumaric acid (1.15 g) in hot ethyl alcohol (10 ml) was added. The precipitate was filtered off to afford N-(2-dimethylaminoethyl)-6-methyl-4-(3-nitrophenyl)-2-phenyl-5-pyrimidinecarboxamide fumarate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698340 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-4212d1f4f87f446797b850813e51097c |
| Source note | uspto-grants-1987_10 |