HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 13923715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-(2-Chloroethyl)-N-(1,1-dimethylethyl)benzenesulfonamide | HCID 15616511 | — |
| Product | HCID 13923715 | HCID 13923715 | 86.6% |
Reaction Steps
The product from Example 14 (15.8 g) was added to 96 ml of trifluoroacetic acid at room temperature. After being stirred for 30 inutes, the reaction mixture yielded white crystals which were collected by filtration, washed well with diethyl ether, and dried to afford 10.9 g of the title compound, m.p. 168°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699650 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-5b6ae2d03820421aa07a878c8471a4fc |
| Source note | uspto-grants-1987_10 |