Fluoride Ion → HCID 13959042, compound

Participants

Reaction Steps

A mixture of 0.35 g of 58B, 3.0 g of Amberlyst A26 fluoride resin and 5 ml of benzene was stirred vigorously at mild reflux in a nitrogen atmosphere overnight. The resulting mixture was filtered, and the filtrate was stripped of solvent. The residue was chromatographed over silica gel, using a 1:99 v:v mixture of ethyl acetate and methylene chloride as eluent, to give 58, as a yellow solid, m.p.: 104°-105° C.

Provenance & Evidence