HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octadecylamine → N-octadecylglucopyranosylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-octadecylglucopyranosylamine | HCID 13361749 | — |
Reaction Steps
20 g of octadecylamine are dissolved in 120 ml of ethanol and the solution is warmed to 70°. 11 g of anhydrous D-glucose are added. After a clear solution has formed, stirring is continued at 70° for a further 15 minutes. The mixture is cooled to 10° and left to stand for 15 minutes. The crystal sludge formed is filtered off with suction, washed twice with ethanol and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699899 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-ace6689b51774ea4845b266b7e04c7b7 |
| Source note | uspto-grants-1987_10 |