HRID255870

反应详情

EQUATION

反应方程式

HRID 255870 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

20 g of octadecylamine are dissolved in 120 ml of ethanol and the solution is warmed to 70°. 11 g of anhydrous D-glucose are added. After a clear solution has formed, stirring is continued at 70° for a further 15 minutes. The mixture is cooled to 10° and left to stand for 15 minutes. The crystal sludge formed is filtered off with suction, washed twice with ethanol and dried in vacuo.

WORKUP

后处理

  1. temperaturethe solution is warmed to 70°
  2. customAfter a clear solution has formed
  3. temperatureThe mixture is cooled to 10°
  4. waitleft
  5. waitto stand for 15 minutes
  6. customThe crystal sludge formed
  7. filtrationis filtered off with suction
  8. washwashed twice with ethanol
  9. customdried in vacuo