HRID255870
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
20 g of octadecylamine are dissolved in 120 ml of ethanol and the solution is warmed to 70°. 11 g of anhydrous D-glucose are added. After a clear solution has formed, stirring is continued at 70° for a further 15 minutes. The mixture is cooled to 10° and left to stand for 15 minutes. The crystal sludge formed is filtered off with suction, washed twice with ethanol and dried in vacuo.
WORKUP
后处理
- temperaturethe solution is warmed to 70°
- customAfter a clear solution has formed
- temperatureThe mixture is cooled to 10°
- waitleft
- waitto stand for 15 minutes
- customThe crystal sludge formed
- filtrationis filtered off with suction
- washwashed twice with ethanol
- customdried in vacuo