HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Alanine → HCID 56616504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Alanine | HCID 239 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | 4-(1H-Imidazol-1-yl)thiophene-2-carbaldehyde | HCID 13318712 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 56616504 | HCID 56616504 | — |
Reaction Steps
A mixture of 94 g 4-(1-imidazolyl)-thiophene-2-aldehyde (EPA 112 987), 47.7 g nitroethane, 4.9 g β-alanine and 327 ml n-butanol is stirred for 9 hours at reflux temperature. Subsequently, it is evaporated and the residue is purified by column chromatography (silica gel//dichloromethane/methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699914 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-faaad6aeea7b43efb81e26b571a0b098 |
| Source note | uspto-grants-1987_10 |