huagongshe.com
HRID256022

反应详情

EQUATION

反应方程式

HRID 256022 的结构方程式

REACTANTS

反应物

2
结构：CNN
HCID6061

Methylhydrazine

CH6N2

结构：CC(C)(C)OC(=O)CN1C(=O)[C@@H](N2C(=O)c3ccccc3C2=O)CSC[C@H]1c1cccs1
HCID13877949

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CN1C(=O)[C@@H](N)CSC[C@H]1c1cccs1
HCID13877951

未命名化合物

收率 90%

PROCEDURE

实验过程

1.18 g of t-butyl α-[5-oxo-6(R)-phthalimido-3(S)-(2-thienyl)perhydro-1,4-thiazepin-4-yl]acetate [prepared as described in step (f) above] was subjected to de-phthaloylization with methylhydrazine in the manner described in Example 1(g), to give 0.77 g of the title compound as an amorphous solid.