HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → t-Butyl alpha-[6-amino-2-(2-naphthyl)-5-oxoperhydro-1,4-thiazepin-4-yl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | t-Butyl alpha-[2-(2-naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate | HCID 20164861 | — |
| Product | t-Butyl alpha-[6-amino-2-(2-naphthyl)-5-oxoperhydro-1,4-thiazepin-4-yl]acetate | HCID 20164805 | 106.9% |
Reaction Steps
3.25 g of t-butyl α-[2-(2-naphthyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetate [prepared as described in step (f) above] were subjected to dephthaloylization with methylhydrazine in the same manner as described in Example 36(g), to give 2.6 g of the title compound as an amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-e2c728d1020f46c6909c1bfb0c6d4d95 |
| Source note | uspto-grants-1987_10 |