huagongshe.com
HRID25607

反应详情

EQUATION

反应方程式

HRID 25607 的结构方程式

REACTANTS

反应物

4
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CCNCCO
HCID8072

2-(Ethylamino)ethanol

C4H11NO

结构：O=C(Cl)Oc1ccc(Cl)cc1
HCID139059

4-Chlorophenyl chloroformate

C7H4Cl2O2

结构：CN[C@H]1CC[C@H](CCCCCOS(C)(=O)=O)CC1
HCID178484796

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CCO)CCCCC[C@H]1CC[C@H](N(C)C(=O)Oc2ccc(Cl)cc2)CC1
HCID178464451

未命名化合物

PROCEDURE

实验过程

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with 2-ethylamino-ethanol to give trans-(4-{5-[Ethyl-(2-hydroxy-ethyl)-amino]-pentyl}-cyclohexyl)-methyl-carbamic acid 4-chloro-phenyl ester, MS: 425 (MH+, 1Cl).