HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → t-Butyl alpha-[2-(2-furyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetat
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | 2-(2-Furyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepine | HCID 13854083 | — |
| Product | t-Butyl alpha-[2-(2-furyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepin-4-yl]acetat | HCID 13854084 | — |
Reaction Steps
Following the procedure described in Example 42(f), 1.15 g of 2-(2-furyl)-5-oxo-6-phthalimidoperhydro-1,4-thiazepine [prepared as described in step (d) above] was treated with t-butyl bromoacetate, to give 0.86 g of the title compound as crystals, melting at 158°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-2cb75d71af9c4868b701e88d62fb3407 |
| Source note | uspto-grants-1987_10 |