HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 13854113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | alpha-{6(R)-[1(S)-ethoxycarbonyl-3-phenylpropylamino]-5-oxo-2-(2-thienyl)perhydro-1,4-thiazepin-4-yl}acetic acid | HCID 13854104 | — |
| Product | HCID 13854113 | HCID 13854113 | 86.3% |
Reaction Steps
The procedure described in Example 44 was repeated, except that 80 mg of α-{6(R)-[1(S)-ethoxycarbonyl-3-phenylpropylamino]-5-oxo-2-(2-thienyl)perhydro-1,4-thiazepin-4-yl}acetic acid (prepared as described in Example 64) were used as the starting material. After hydrolysis of the starting material with sodium hydroxide, 65 mg of the title compound were obtained as a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699905 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-467f9ff619064c4ca280a80ad94578f6 |
| Source note | uspto-grants-1987_10 |