HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,3,5-Trifluoropyridin-4-yl)methanol → HCID 86741836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,3,5-Trifluoropyridin-4-yl)methanol | HCID 13985162 | — |
| Reactant | cis-3-(2-Chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride | HCID 86737382 | — |
| Product | HCID 86741836 | HCID 86741836 | 45.1% |
Reaction Steps
By the method of Example 2, 0.3 g (0.002 mole) of 4-hydroxymethyl-2,3,5-trifluoropyridine (from Example 9) was reacted with 0.5 g (0.002 mole) of cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride to produce 0.35 g of (2,3,5-trifluoropyridin-4-yl)methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate as a clear, yellow oil, Compound 15 of the tables below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04701464 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-1172845dfea74231973f73aa88cc26bc |
| Source note | uspto-grants-1987_10 |