HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)-6-fluoropyridine → 2-Bromoethyl-6-fluoropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)-6-fluoropyridine | HCID 13985218 | — |
| Reactant | 2-(Dibromomethyl)-6-fluoropyridine | HCID 20164237 | — |
| Product | 2-Bromoethyl-6-fluoropyridine | HCID 20164232 | — |
Reaction Steps
Fractions 2 and 3 were >96% pure 2-bromomethyl-6-fluoropyridine and were therefore combined. Fraction 4 was composed of a 1:1 mixture of 2-bromomethyl-6-fluoropyridine and 2-dibromomethyl-6-fluoropyridine. The nmr spectra was consistent with the proposed structure for Fractions 2 and 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04701464 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-8768866ccc434663906aa8f5a0dc546b |
| Source note | uspto-grants-1987_10 |