Thioglycolic Acid → HCID 86111447, compound

HRID 256236Notes

Reaction equation

HRID 256236 reaction equation
[C:1]1([CH2:7][CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[SH:10][CH2:11][C:12](O)=[O:13].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[C:1]1([CH2:7][CH2:8][O:9][C:12](=[O:13])[CH2:11][SH:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 1133Thioglycolic AcidHCID 60542-PhenylethanolHCID 6101p-Toluenesulfonic acid

Product 1

HCID 86111447HCID 86111447, compound

Procedure

Into a 100 ml reaction flask equipped with thermometer, reflux condenser, hot plate (with magnetic stirring apparatus included within) and spin bar are placed 12.2 grams of phenylethyl alcohol; 23.0 grams mercaptoacetic acid; and 0.5 grams of para-toluene sulphonic acid.

Workup

  1. customInto a 100 ml reaction flask
  2. customequipped with thermometer
  3. temperaturereflux condenser

Sources & evidence

ORD record
ord-cb462d6007ea41e1baa0f16f2227a741
Source dataset
uspto-grants-1987_10
Patent number
US04701548

Reaction notes

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