Thioglycolic Acid → HCID 53859405, compound

HRID 256237Notes

Reaction equation

HRID 256237 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][OH:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[SH:11][CH2:12][C:13](O)=[O:14].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[SH:11][CH2:12][C:13]([O:10][CH2:9][CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:14]

Participants

4

Reactant 3

HCID 1133Thioglycolic AcidHCID 6101p-Toluenesulfonic acidHCID 31234Benzenepropanol

Product 1

HCID 53859405HCID 53859405, compound

Procedure

Into a 100 ml flask equipped with reflux condenser, thermometer, hot plate (including magnetic stirring apparatus within) and spin bar are placed 13.6 grams phenylpropyl alcohol; 4 grams of mercaptoacetic acid; and 0.1 grams para-toluene sulphonic acid.

Workup

  1. customInto a 100 ml flask equipped
  2. temperaturewith reflux condenser

Sources & evidence

ORD record
ord-4c2e40cdece84ae2a87cb6be30cd2548
Source dataset
uspto-grants-1987_10
Patent number
US04701548

Reaction notes

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