HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyloxycarbonylglycine → HCID 20163746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyloxycarbonylglycine | HCID 14349 | — |
| Reactant | 2,2,5-Trimethylimidazolidin-4-one | HCID 13443912 | — |
| Product | HCID 20163746 | HCID 20163746 | — |
Reaction Steps
The same procedure of the Example 2, starting from N-benzyloxycarbonylglycine and 2,2,5-trimethyl-4-imidazolidinone (m.p. 74°-75° C.; obtained from DL-alaninamide and acetone), afforded 1-(2-benzyloxycarbonylaminoacetyl)-2,2,5-trimethyl-4-imidazolidinone, m.p 170°-171° C., then the title compound m.p. 161°-163° C. dec. Mass spectrum (C.I., i--C4H10, 70 eV, 1.5 mA), m/z=186 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703054 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-bf83f67b234f450985f73dc33b8921cc |
| Source note | uspto-grants-1987_10 |