HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-(2-Acetamidoacetyl)-2,2-dimethyl-4-imidazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1-(2-Aminoacetyl)-2,2-dimethyl-4-imidazolidinone | HCID 20163713 | — |
| Product | 1-(2-Acetamidoacetyl)-2,2-dimethyl-4-imidazolidinone | HCID 20163708 | — |
Reaction Steps
A suspension of 1-(2-aminoacetyl)-2.2-dimethyl-4-imidazolidinone (5 g) in acetic anhydride (20 ml) was stirred at room temperature for 1 hour. Evaporation under vacuum and crystallization of the residue from 2-propanol gave 4.63 g of the title compound, m.p. 214°-215° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703054 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-9e503bd0e6b64536b7061cc7c8bfff86 |
| Source note | uspto-grants-1987_10 |