HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanone, 2-benzofuranylphenyl- → HCID 13728724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanone, 2-benzofuranylphenyl- | HCID 95808 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13728724 | HCID 13728724 | 92.3% |
Reaction Steps
To a solution of 22 g (0.1 mole) of 2-benzoylbenzo(b)furan in 250 ml acetic acid was added 3 g 10% Pd/C catalyst and the mixture hydrogenated at 3 atmospheres pressure, with shaking for 70 hours. The mixture was filtered and the filtrate concentrated in vacuo to obtain 19.4 g (92%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703052 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-18d4b4c696db47d2888cd9fbb6e52677 |
| Source note | uspto-grants-1987_10 |