Triethylsilane → HCID 13728725, compound

Participants

Reaction Steps

Reduction of 15 g (86.0 mmole) of the above product with triethylsilane in trifluoroacetic acid by the method of Preparation D, Part (iv), and purification of the crude product on a silica gel column, eluting with hexane and hexane containing 5% ethyl acetate and distillation of the combined product fractions gave 15.5 g of the title compound as a clear oil, b.p. 114°-120° C. 15 Torr. M.S. (m/e): 176 (M+), TLC Rf 0.55, hexane.

Provenance & Evidence