HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 10243414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | p-Xylyl bromide | HCID 7721 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10243414 | HCID 10243414 | — |
Reaction Steps
The procedure of Example 1 is repeated using 10.6 g of sodium carbonate, 1.74 g of hydroxylamine hydrochloride and 9.25 g of p-methylbenzyl bromide in 50 ml of dimethylformamide. Trituration of the crude product with ethanol affords 3.3 g of the above-named hydroxylamine as a white solid, mp 107°-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04703073 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-7851a5283465458ba1fbc0c8fe41aa71 |
| Source note | uspto-grants-1987_10 |