Hydrochloric Acid → HCID 53977328, compound

HRID 256464Notes

Reaction equation

HRID 256464 reaction equation
[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]=[O:6].Cl.[C:8](=[O:11])([O-])[O-].[Na+].[Na+].[CH3:14]O>>[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]([O:11][CH3:8])[O:6][CH3:14]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 887MethanolHCID 10340Sodium CarbonateHCID 537074664-Chlorobut-2-enal

Product 1

HCID 53977328HCID 53977328, compound

Procedure

4-Chloro-1,1-dimethyoxy-2-butene (Reagent K) was prepared by reacting 7.46 g. of 4-chloro-2-butenal with 200 ml. of anhydrous methanol and a catalytic amount of hydrochloric acid. The reaction mixture was stirred at room temperature for 16 hours, neutralized with sodium carbonate, filtered, and concentrated.

Workup

  1. filtrationfiltered
  2. concentrationconcentrated

Sources & evidence

ORD record
ord-063d2bb45b8947eda8c257c5d731e7ae
Source dataset
uspto-grants-1987_10
Patent number
US04703116

Reaction notes

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