HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene Oxide → HCID 19785211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | HCID 19785210 | HCID 19785210 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19785211 | HCID 19785211 | — |
Reaction Steps
A mixture of 2-(1-phenylsulphonyl-3-pyrrolyl)ethylamine (1.8 g), styrene oxide (0.51 g) and acetonitrile (20 ml) were refluxed for three days. The solution was evaporated and the brown oil was purified by chromatography on silica, eluting with dichloromethane, chloroform then with increasing amounts of methanol (1→10%) in chloroform, to give the title product as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05258378 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-f8b98f00d24948a5ba76f772092d31ce |
| Source note | uspto-grants-1993_11 |