HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene Oxide → HCID 19785208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | HCID 19785209 | HCID 19785209 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19785208 | HCID 19785208 | — |
Reaction Steps
A mixture of N-methyl-2-(1-phenylsulphonyl-3-pyrrolyl)ethylamine (4 g), styrene oxide (2.06 g) and acetonitrile (50 ml) were refluxed for 2 days. The solution was evaporated and the brown oil was purified by chromatography on silica, eluting with dichloromethane, chloroform then with increasing amounts of methanol (1→25%) in chloroform to give the title product as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05258378 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-63bd212717c74b53b32b1480fba84c1d |
| Source note | uspto-grants-1993_11 |