HCID 53983035, compound → HCID 86747349, compound

Participants

Reaction Steps

2.71 g (10.0 mmol) of 2,6-bis(dimethylaminomethylene)phenyl bromide in 40 ml of hexane, 6.3 ml of n-butyllithium (10.0 mmol; 1.6 mol/l in hexane) and 1.8 g (10.0 mmol) of dimethylindium chloride in 20 ml of hexane are reacted analogously to Example 1 to give [2,6-bis(di-methylaminomethylene)phenyl] dimethylindium, which is obtained in the form of colorless crystals, m.p. 53° C., by cooling a concentrated hexane solution to -30° C.

Provenance & Evidence