HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54293641, compound → HCID 86747350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54293641 | HCID 54293641 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178461624 | HCID 178461624 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86747350 | HCID 86747350 | — |
Reaction Steps
2.4 g (7.3 mmol) of 2,6-bis(diethylaminomethylene)phenyl bromide in 40 ml of hexane, 4.6 ml of butyllithium (7.3 mmol; 1.6 mol/l in hexane) and 1.5 g (7.3 mmol) of diethylindium chloride in 20 ml hexane are reacted analogously to Example 1 to give [2,6-bis(diethylaminomethylene)phenyl]diethylindium, which is obtained as a colorless liquid, b.p. 115° C./0.04 mbar, by vacuum distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05259915 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-3a6792b2a97f420a80d370938b1feeb0 |
| Source note | uspto-grants-1993_11 |