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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 256787Generated: October 31, 2026

HCID 54293641, compound → HCID 86747350, compound

https://huagongshe.com/reaction/256787

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54293641HCID 54293641—
ReactantButyllithiumHCID 178418339—
ReactantHCID 178461624HCID 178461624—
SolventHexaneHCID 8058—
ProductHCID 86747350HCID 86747350—

Reaction Steps

2.4 g (7.3 mmol) of 2,6-bis(diethylaminomethylene)phenyl bromide in 40 ml of hexane, 4.6 ml of butyllithium (7.3 mmol; 1.6 mol/l in hexane) and 1.5 g (7.3 mmol) of diethylindium chloride in 20 ml hexane are reacted analogously to Example 1 to give [2,6-bis(diethylaminomethylene)phenyl]diethylindium, which is obtained as a colorless liquid, b.p. 115° C./0.04 mbar, by vacuum distillation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05259915
Source datasetuspto-grants-1993_11
ORD IDord-3a6792b2a97f420a80d370938b1feeb0
Source noteuspto-grants-1993_11