HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19784262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19784270 | HCID 19784270 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19784262 | HCID 19784262 | 77.1% |
Reaction Steps
Using the procedure described in example 19 but starting with 3-{2-[4-(4-fluorophenyl)-1-piperazinyl]ethyl}-2-trifluoroacetylimino-6-trifluoromethylbenzothiazoline (3.5 g), a 7% strength aqueous alcoholic solution (15 cc) of potassium carbonate and methanol (150 cc). 2-imino-3-{2-[4-(4-fluorophenyl)-1-piperazinyl]ethyl}-6-trifluoromethylbenzothiazoline (2.2 g) m.p. 250° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260297 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-2ab4fd29fd08470282dfc73f58ff8b42 |
| Source note | uspto-grants-1993_11 |