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HRID256838

反应详情

EQUATION

反应方程式

HRID 256838 的结构方程式

REACTANTS

反应物

2
结构：Brc1cc2ccccc2s1
HCID94786

Benzo(b)thiophene, 2-bromo-

C8H5BrS

结构：C#CC1(C)CCc2c(C)c(O)c(C)c(C)c2O1
HCID14478563

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(C)c2c(c(C)c1O)CCC(C)(C#Cc1cc3ccccc3s1)O2
HCID15171820

未命名化合物

PROCEDURE

实验过程

Reaction of rac-3,4-dihydro-2-ethynyl-2,5,7,8-tetramethyl-2H-1-benzopyran-6-ol with 2-bromobenzo[b]thiophene under the conditions described in example 16 gave after chromatographic isolation and crystallization from ether/hexane colorless crystals with m.p. 120°-123° C.

WORKUP

后处理

  1. customgave
  2. customafter chromatographic isolation and crystallization from ether/hexane colorless crystals with m.p. 120°-123° C.