Iodoethane → HCID 19075330, compound

HRID 256950Notes

Reaction equation

HRID 256950 reaction equation
[Cl:1][C:2]1[C:3]([C:7]2[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=2)=[N:4][S:5][N:6]=1.[CH2:13]([I:15])[CH3:14]>CC(C)=O>[I-:15].[Cl:1][C:2]1[C:3]([C:7]2[CH:8]=[N+:9]([CH2:13][CH3:14])[CH:10]=[CH:11][CH:12]=2)=[N:4][S:5][N:6]=1

Participants

4

Reactant 2

HCID 6340IodoethaneHCID 104881643-Chloro-4-(pyridin-3-yl)-1,2,5-thiadiazole

Product 1

HCID 19075330HCID 19075330, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A solution of 3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine (1.13 g, 5.7 mmol) and ethyl iodide (22.65 g, 17 mmol) in acetone (15 ml) was stirred at 40° C. for 16 h. The precipitate was collected by filtration giving the title compound. Yield: 510 mg (26%).

Workup

  1. filtrationThe precipitate was collected by filtration

Sources & evidence

ORD record
ord-6a7cedb4c72645a8a4e40968545a8866
Source dataset
uspto-grants-1993_11
Patent number
US05260311

Reaction notes

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