HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(3-(3-Pentynyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-(3-Pentynyloxy)-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075260 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(3-(3-Pentynyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075240 | — |
Reaction Steps
A mixture of methyl iodide (0.6 ml, 9 mmol) and 3-(4-(3-pentynyloxy)-1,2,5-thiadiazol-3-yl) pyridine (3 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.68 g (59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260311 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-cd925a1936684902971eddc784973986 |
| Source note | uspto-grants-1993_11 |