4-Chloro-N-(pentan-2-yl)benzamide → HCID 15086158, compound

HRID 257074Notes

Reaction equation

HRID 257074 reaction equation
[CH3:1][CH:2]([NH:6][C:7](=O)[C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=1)[CH2:3][CH2:4][CH3:5]>C1COCC1>[CH3:1][CH:2]([NH:6][CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][CH:9]=1)[CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 1

HCID 3467014-Chloro-N-(pentan-2-yl)benzamide

Product 1

HCID 15086158HCID 15086158, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

In a manner analogous to Example 1 a solution of N-(1-methylbutyl)-4-chlorobenzamide (2.26 g; 0.01 mol) in dry THF (25 ml) was reacted with an ice-cooled solution of 1.0 M.B2H6 -THF complex (45 ml; 0.045 mol) under a nitrogen blanket to give the title compound as an oil.

Workup

  1. temperaturecooled solution of 1.0 M

Sources & evidence

ORD record
ord-ea48770cb8ab410995e9dd5fdd59c97b
Source dataset
uspto-grants-1993_11
Patent number
US05260331

Reaction notes

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