HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 19784361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 19784357 | HCID 19784357 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19784361 | HCID 19784361 | — |
Reaction Steps
1.9 g (6.1 mmol) of the base of the product from Example 23 were reduced with 1.1 g (9.2 mmol) of triethylsilane and 8.0 g of glacial acetic acid in a similar manner to Example 14. 2.0 g of 4-(N-benzyl-N-methylamino)-1-(4-tolyl)piperidine fumarate were obtained. Melting point 161°-163° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260318 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-477505b97f83452280cdd3f35a040b14 |
| Source note | uspto-grants-1993_11 |