Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 4-n-Octylphenol | HCID 15730 | — |
| Product | HCID 6429813 | HCID 6429813 | 85% |
Reaction Steps
The procedure described in Example 4 was followed, replacing the phenol (48 g) by 4-octylphenol (105 g 0.5 mole). During addition of the paraformaldehyde, the internal temperature was maintained at 95°-98° C. and the reaction mixture was stirred at 98° C. for a further hour. In other respects, the conditions were as described in Example 4. The product, 5-octylsalicylaldehyde, was obtained in 85% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05260487 |
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| Source dataset | uspto-grants-1993_11 |
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| ORD ID | ord-2bb42aa5a41649d8a726326cca3fa785 |
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| Source note | uspto-grants-1993_11 |
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