HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylpyridine → 1-(2,4-Dichlorophenyl)-3-(4-pyridyl)butane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylpyridine | HCID 10822 | — |
| Reactant | 2,4-Dichlorophenethyl bromide | HCID 10848510 | — |
| Product | 1-(2,4-Dichlorophenyl)-3-(4-pyridyl)butane | HCID 19783332 | 25.6% |
Reaction Steps
1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,4-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.67 g of the desired compound (yield: 25.6%). The resulting compound was identified as 1-(2,4-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 9) by the following analytical results.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262420 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-985276f4426647a1a82ad766a78c1cc0 |
| Source note | uspto-grants-1993_11 |