Phenethyl bromide → HCID 466133, compound

HRID 257470Notes

Reaction equation

HRID 257470 reaction equation
[CH3:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1[CH3:8].[CH2:9](Br)[CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([CH2:10][CH2:9][CH2:8][C:7]2[CH:6]=[CH:5][N:4]=[CH:3][C:2]=2[CH3:1])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 7666Phenethyl bromideHCID 114173,4-Dimethylpyridine

Product 1

HCID 466133HCID 466133, compoundYield 92.4%

Procedure

1.0 g (9.35 mmol) of 3,4-dimethylpyridine and 1.73 g (9.35 mmol) of phenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.82 g of the desired compound (yield: 92.4%).

Workup

  1. customThe reaction product was purified

Sources & evidence

ORD record
ord-3cac0c5093bc40ad89b9a00e846199bd
Source dataset
uspto-grants-1993_11
Patent number
US05262420

Reaction notes

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