HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethylpyridine → 1-(3-Chlorophenyl)-4-(3-methyl-4-pyridyl) butane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethylpyridine | HCID 11417 | — |
| Reactant | 1-(3-Bromopropyl)-3-chlorobenzene | HCID 14084860 | — |
| Product | 1-(3-Chlorophenyl)-4-(3-methyl-4-pyridyl) butane | HCID 14883794 | 45.7% |
Reaction Steps
1.0 g (9.35 mmol) of 3,4-dimethylpyridine and 2.18 g (9.35 mmol) of 1-bromo-3-(3-chlorophenyl)-propane were reacted in the same manner as in Example 26. The reaction product was purified to obtain 1.11 g of the desired compound (yield: 5.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262420 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-06c1c521d1b5456fa9c2c71a0f15490f |
| Source note | uspto-grants-1993_11 |