HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethyl-4-methylpyridine → 1-(3,4-Dichlorophenyl)-4-(3-ethyl-4-pyridyl)-butane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethyl-4-methylpyridine | HCID 68254 | — |
| Reactant | 4-(3-bromopropyl)-1,2-dichloroBenzene | HCID 21962957 | — |
| Product | 1-(3,4-Dichlorophenyl)-4-(3-ethyl-4-pyridyl)-butane | HCID 14883797 | 46.9% |
Reaction Steps
1.83 g (15.1 mmol) of 3-ethyl-4-methypyridine and 4.05 g (15.1 mmol) of 1-bromo-3-(3,4-dichlorophenyl)-propane were reacted in the same manner as in Example 26. The reaction product was purified to obtain 2.18 g of the desired compound (yield: 46.9%). The resulting compound was identified as 1-(3,4-dichlorophenyl)-4-(3-ethyl-4-pyridyl)-butane (hereinafter referred to as compound 51) by the following analytical results.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262420 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-7066780fb54943e7af17fba3eed20548 |
| Source note | uspto-grants-1993_11 |