HRID257746

反应详情

EQUATION

反应方程式

HRID 257746 的结构方程式

PROCEDURE

实验过程

The 5-(5-bromobutyryl)-8-chloro-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one, used as starting material, is synthesized similarly to the starting material described in Example 1 from 8-chloro-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one and 4-bromobutyryl chloride. The yield is 83.1% of the theoretical yield and the melting point is 176°-177° C.

WORKUP

后处理

  1. customis synthesized similarly to the starting material
  2. customThe yield is 83.1% of the theoretical yield