HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Bromobutyryl chloride → 8-Chloro-5-(4-diethylamino-butyryl)-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Bromobutyryl chloride | HCID 70225 | — |
| Edukt | 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 3653116 | — |
| Produkt | 8-Chloro-5-(4-diethylamino-butyryl)-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one | HCID 10667837 | — |
Reaktionsschritte
The 5-(5-bromobutyryl)-8-chloro-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one, used as starting material, is synthesized similarly to the starting material described in Example 1 from 8-chloro-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one and 4-bromobutyryl chloride. The yield is 83.1% of the theoretical yield and the melting point is 176°-177° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05264432 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-d3b24c7feeb842ad93fc96aa34fb579e |
| Quellennotiz | uspto-grants-1993_11 |