HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19781545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15170433 | HCID 15170433 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 19781545 | HCID 19781545 | 90% |
Reaction Steps
Concentrated hydrochloric acid (0.23 g; 2.2 mmoles) was added to an ethanol/methylene chloride solution of 2-(4-diphenylmethylpiperazino)-5,6-dihydro-7-methyl-6-oxo(7H)pyrrolo[2,3-d]pyrimidine, and the solution was stirred at room temperature for 1 hour. The solvent was then evaporated under reduced pressure. The residue was washed with ether to give 0.88 g (yield 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05264435 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-ab98bb173ebc4a8d8b021fb4cd6acf9b |
| Source note | uspto-grants-1993_11 |