p-Toluenesulfonic acid → HCID 19781549, compound

Participants

Reaction Steps

An ethyl acetate/methanol solution of 0.13 g (0.75 mmole) of p-toluenesulfonic acid was added to an ethyl acetate/methanol solution of 0.31 g (0.75 mmole) of 2-(4-(α(4-methylphenyl)benzyl)piperazino)-5,6-dihydro-7-methyl-6-oxo(7H)pyrrolo[2,3-d]pyrimidine, and the mixture was stirred at room temperature for 1 hour. The solvents were then evaporated under reduced pressure, and the residue was washed with hexane to give 0.36 g (yield 81%) of the desired compound.

Provenance & Evidence