HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19075336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19075253 | HCID 19075253 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19075336 | HCID 19075336 | — |
Reaction Steps
A mixture of methyl iodide (0.45 ml, 7.2 mmol) and 3-(4-propargyloxy-1,2,5-thiadiazol-3-yl)pyridine (430 mg, 2.4 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.58 g (67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05264444 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-98dc995d3dd748c497230d02eb1f51c7 |
| Source note | uspto-grants-1993_11 |