HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22446990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1-(Bromomethyl)-3-(trifluoromethyl)benzene | HCID 123061 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22446990 | HCID 22446990 | — |
Reaction Steps
A solution of 3-trifluoromethylbenzylbromide (4.6 g, 0.019 mol) and triphenylphosphine (5.0 g, 0.019 mol) in dry toluene (200 mL) was heated to reflux for two hours. The precipitate was filtered off by suction, washed with toluene, and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05266593 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-4dd6f185958a426581467bc4c5fc3c0e |
| Source note | uspto-grants-1993_11 |