HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 6-Diethylphosphono-3-methyl-2,4-hexadienal dioxolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 2-Bromo-1,3-dioxolane | HCID 14372566 | — |
| Product | 6-Diethylphosphono-3-methyl-2,4-hexadienal dioxolane | HCID 86747400 | — |
Reaction Steps
Triethyl phosphite (2.56 g, 15.44 mmol) in dry toluene (10 ml) and bromodioxolane (H) (3 g, 12.87 mmol) in toluene (10 ml) were introduced in succession into a 50-ml two-necked flask fitted with a thermometer and a condenser.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05266708 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-cd82384b784d4ebca17d40c0c996320e |
| Source note | uspto-grants-1993_11 |