HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 178504101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 14364274 | HCID 14364274 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178504101 | HCID 178504101 | — |
Reaction Steps
To a solution of 2.3 parts of diethyl (methylthio)thiocarbonylphosphonate in 50 parts of dry tetrahydrofuran was added 1.5 parts of sodium iodide. The solution was stirred for 18 hours at room temperature, then warmed on a steam bath for one-half hour. The desired orange ethyl sodium (methylthio)thiocarbonylphosphonate was then filtered, m.p. 288° d.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04033749 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-c4a904e984e44e558650cd8179fd3d6d |
| Source note | uspto-grants-1977_07 |