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HRID258539

反应详情

EQUATION

反应方程式

HRID 258539 的结构方程式

REACTANTS

反应物

2
结构：S=P12SP3(=S)SP(=S)(S1)SP(=S)(S2)S3
HCID14817

Phosphorus pentasulfide

P4S10

结构：O=C1CC(=O)N(c2ccccc2)c2cc(Cl)ccc2N1
HCID89657

N-Desmethylclobazam

C15H11ClN2O2

PRODUCTS

生成物

1
结构：O=C1CC(=S)Nc2ccc(Cl)cc2N1c1ccccc1
HCID12264319

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

A solution of 28.6 g of 7-chloro-5-phenyl-1H-1,5-benzodiazepine-2,4-dione and 23.3 g of phosphorus pentasulfide in 250 ml of pyridine is refluxed, with stirring, for 40 minutes under argon. The solvent is evaporated in vacuo.

WORKUP

后处理

  1. customThe solvent is evaporated in vacuo