HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycerol → HCID 68125393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68125393 | HCID 68125393 | — |
Reaction Steps
A mixture of p-menth-3-oyl chloride (2 g.) and glycerol (20 ml.) was heated at 100° for 4 hours. The mixture was then poured into water (600 ml.) and extracted 3 times with ether. The extracts were dried (MgSO4) and the solvent removed under reduced pressure to leave 1,2-bis-(p-menth-3-oyl)glycerol as a colourless oil (1.2 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04033994 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-2cce7e969fd3433e9bccccdf5a4e3333 |
| Source note | uspto-grants-1977_07 |