Catechol → HCID 21426269, compound

HRID 258591Notes

Reaction equation

HRID 258591 reaction equation
[CH:1]1([CH3:13])[CH2:6][CH2:5][CH:4]([CH:7]([CH3:9])[CH3:8])[CH:3]([C:10](Cl)=[O:11])[CH2:2]1.[C:14]1([C:16](=[CH:18][CH:19]=[CH:20][CH:21]=1)[OH:17])[OH:15]>C1(C)C=CC=CC=1>[CH:1]1([CH3:13])[CH2:6][CH2:5][CH:4]([CH:7]([CH3:9])[CH3:8])[CH:3]([C:10]([O:15][C:14]2[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=2[OH:17])=[O:11])[CH2:2]1

Participants

4

Reactant 2

HCID 289CatecholHCID 13734319Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)-

Product 1

HCID 21426269HCID 21426269, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

p-Menth-3-oyl chloride (2.0 g.) and pyrocatechol (1.1 g.) were heated under refluxing conditions in toluene (75 ml.) for 4 hours. An oily liquid was recovered which was identified as ortho-hydroxyphenyl p-menthane-3-carboxylate.

Workup

  1. customAn oily liquid was recovered which

Sources & evidence

ORD record
ord-6bac1f51bb4542d4ba42d21cd07c2d52
Source dataset
uspto-grants-1977_07
Patent number
US04033994

Reaction notes

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